文献类型: 外文期刊
作者: Wei, Hailian 1 ; Yang, Xianglong 1 ; Cheng, Ling 1 ; Zhang, Qi 1 ; Mao, Jin 1 ; Li, Peiwu 1 ;
作者机构: 1.Chinese Acad Agr Sci, Oil Crops Res Inst, Wuhan 430062, Peoples R China
2.Minist Agr, Natl Reference Lab Agr Testing PR China, Lab Qual & Safety Risk Assessment Oilseed Prod Wuh, Key Lab Detect Mycotoxins,Key Lab Biol & Genet Imp, Wuhan, Peoples R China
关键词: Accurate quantification; Efficient extraction; Gas chromatography-mass spectrometry; Risk assessment; Response surface methodology
期刊名称:FOOD CHEMISTRY ( 影响因子:9.8; 五年影响因子:9.7 )
ISSN: 0308-8146
年卷期: 2025 年 468 卷
页码:
收录情况: SCI
摘要: Phthalic acid esters (PAEs), widely used in food processing, pose significant risks to food safety and human health. A rapid and accurate method to simultaneously detect 18 PAEs in edible oil was developed and applied to evaluate daily exposures in Hubei. By using ultrasound-assisted extraction and GC-MS with deuterated isotopes, we improved extraction efficiency and detection accuracy. The method exhibited excellent linearity and low limits of quantification, with average recoveries ranging from 84.32 % to 115.80 % and relative standard deviations between 2.08% and 12.82%. Among 30 commercial edible oils analyzed, higher average levels of DBP, DEHP, and DINP were found at 0.207, 1.767, and 0.600 mg/kg, respectively. Dietary exposure assessment indicated that daily intakes were below health guideline values, but DEHP posed a relatively higher health risk. These findings provide a simple method and reference for assessing PAEs exposure and health risk in edible oil.
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