Effervescence-assisted salting-out liquid-liquid extraction for rapid and convenient analysis of pyrethroid pesticide residues
文献类型： 外文期刊
作者： Li, Wenxuan 1 ; Xu, Yaxi 2 ; Wang, Meifei 1 ; Wang, Yuyang 1 ; Wei, Jinchao 3 ; Chen, Di 1 ;
作者机构： 1.Zhengzhou Univ, Sch Pharmaceut Sci, Natl Key Lab Cotton Biobreeding & Integrated Utili, Henan Key Lab Nanomed Targeting Diag & Treatment, Zhengzhou 450001, Henan, Peoples R China
2.Chinese Acad Agr Sci, Oil Crops Res Inst, Wuhan 430062, Peoples R China
3.Univ Macau, Inst Chinese Med Sci, Macau Ctr Res & Dev Chinese Med, State Key Lab Qual Res Chinese Med, Macau 999078, Peoples R China
关键词： Salting-out assisted liquid-liquid extraction; Effervescence; Pyrethroid insecticides; Gas chromatography with an electron capture; detector; Juices; Herbal extract
期刊名称：TALANTA （ 影响因子：6.1； 五年影响因子：5.5 ）
ISSN： 0039-9140
年卷期： 2025 年 287 卷
页码：
收录情况： SCI
摘要： A simple and efficient effervescence-assisted salting-out assisted liquid-liquid extraction (EA-SALLE) method was developed for the rapid extraction of pyrethroid insecticides in fruit juices and herbal extracts. By integrating effervescence extraction with SALLE, the extraction and phase separation processes were conducted simultaneously, significantly simplifying the experimental procedure and reducing the extraction time to just 3 min. Key factors influencing the method's efficiency were systematically optimized. Combined with gas chromatography with an electron capture detector, enabled the determination of nine pyrethroid insecticides, demonstrating excellent linearity (R-2 > 0.99), low limits of detection (0.03-0.17 ng/mL), satisfactory accuracy (recoveries ranging from 83.0 % to 107.9 %), and good precision (RSD < 9.1 %). The proposed EA-SALLE method offers a simple, efficient, and cost-effective sample preparation technique. It is characterized by ease of operation, short extraction time, and high sensitivity, providing an effective tool for the monitoring and assessment of pesticide residues in complex samples.
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