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Synthesis of E-beta-farnesene analogues containing five-membered azaheterocycles and their biological activity

文献类型： 外文期刊

作者： Kang Tie-Niu 1 ; Ling Yun 1 ; Rui Chang-Hui 2 ; Yang Xin-Ling 1 ; Fan Xian-Lin 2 ; Chen Fu-Heng 1 ;

作者机构： 1.China Agr Univ, Dept Appl Chem, Beijing 100094, Peoples R China

2.Chinese Acad Agr Sci, Inst Plant Protect, Beijing 100094, Peoples R China

关键词： azaheterocycle;EBF analogue;synthesis;biological activity

期刊名称：CHINESE JOURNAL OF ORGANIC CHEMISTRY （ 影响因子：1.652； 五年影响因子：1.2 ）

ISSN： 0253-2786

年卷期： 2008 年 28 卷 4 期

页码：

收录情况： SCI

摘要： In order to find novel leading compounds used to control aphids, eight E-beta-farnesene (EBF) analogues were synthesized from the skeletal structure of EBF, the main component of aphid alarm pheromones, where the conjugate double bond was superseded by nitrogen heterocyclic compounds such as N-nitroimidazolidin-2-imine, thiazolidine-2-thione, oxazolidin-2-one, etc. The structures of all the target compounds were confirmed by (1)H NMR, IR spectra and elemental analysis, and the different reaction and biological activities of these compounds were also discussed. The results of biological tests indicated that most compounds showed insecticidal activity against Lipaphis erysimi, especially the inhibition rate of 4e was higher than that of thiacloprid at testing five concentrations. The interesting phenomenon is that at a lower concentration (e.g. 62.5 mu g/mL), the inhibition rate of most compounds is better than that of thiacloprid despite that they are worse than thiacloprid at 1000 mu g/mL.

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