您好，欢迎访问中国农业科学院 机构知识库！

全部

  • 全部
  • 标题
  • 学者
  • 机构
  • 关键词

Simultaneous Determination of 14 Kinds of beta-Agonist Residues in Sheep Saliva by Ultra Performance Liquid Chramatogrephy-Tandem Mass Spectrometry

文献类型： 外文期刊

作者： Li Yang 1 ; Su Xiao-Ou 1 ; Wang Rui-Guo 1 ; Wang Pei-Long 1 ; Zhang Wei 1 ; Chen Jie 1 ;

作者机构： 1.Chinese Acad Agr Sci, Inst Qual Stand & Testing Technol Agroprod, Beijing 100081, Peoples R China

关键词： beta-Agonist;Saliva;Solid phase extraction;Ultra performance liquid chromatography-tandem mass spectrometry

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2013 年 41 卷 6 期

页码：

收录情况： SCI

摘要： A sensitive method was developed for the determination of 14 kinds of beta-agonists residues in sheep saliva by solid phase extraction pretreatment and ultra performance liquid chromatography tandem mass spectrometry. The sample was adjusted by pH5. 2 ammonium acetate buffer and centrifuged separation to eliminate impurity, then passed through MCX cartridge to clear-up. The test potion was separated by waters BEH C-18 columns with gradient elution program. Analyte confirmation was performed using multiple reaction monitoring (MRM) with one precursor ion and productions as identifiers. The results were calculated by internal standard method. The LODs were 0. 1-0. 2 mu g/L, LOQs were 0. 3-0. 5 mu g/L, the recoveries were in range of 60% - 110%, and the relative standard deviations (RSDs) were less than 20% at three spiked levels for beta-agonists.

  • 相关文献

[1]Host plant effects on alkaline phosphatase activity in the whiteflies, Bemisia tabaci Biotype B and Trialeurodes vaporariorum. Peng, Lu,Liu, Wan-Xue,Wan, Fang-Hao,Peng, Lu,Harris, Marvin K.. 2011

[2]Age- and sex-associated differences in the glycopatterns of human salivary glycoproteins and their roles against influenza A virus. Qin, Yannan,Zhong, Yaogang,Zhu, Minzhi,Dang, Liuyi,Yu, Hanjie,Chen, Zhuo,Chen, Wentian,Li, Zheng,Wang, Xiurong,Zhang, Hua.

[3]Identification, comparison, and functional analysis of salivary phenol-oxidizing enzymes in Bemisia tabaci B and Trialeurodes vaporariorum. Peng, Lu,Yan, Ying,Yang, Chun Hong,Wan, Fang Hao,Peng, Lu,De Barro, Paul J.. 2013

[4]A sensitive and quantitative fluorescent multi-component immuno-chromatographic sensor for beta-agonist residues. Wang, Peilong,Su, Xiaoou,Wang, Peilong,Su, Xiaoou,Wang, Zhi.

[5]Cell-Free Expression, Purification, and Characterization of the Functional beta(2)-Adrenergic Receptor for Multianalyte Detection of beta-Agonists. Wang, Jian,Liu, Yuan,Han, Zhengzheng,Wang, Wei,Liu, Yang,Wei, Dong,Wang, Jian,Liu, Yuan,Zhang, Junhua,Huang, Wei. 2017

[6]Direct measurement of beta-agonists in swine hair extract in multiplexed mode by surface-enhanced Raman spectroscopy and microfluidic paper. Dou, Bin,Luo, Yong,Gao, Zhigang,Zhao, Weijie,Lin, Bingcheng,Dou, Bin,Luo, Yong,Gao, Zhigang,Zhao, Weijie,Chen, Xu,Shi, Bo,Du, Yuguang,Lin, Bingcheng.

[7]Determination of Glyphosate, Aminomethyl Phosphonic Acid and Glufosinate in Different Teas by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry. Zhu Li,Chen Hong-Ping,Zhou Su-Juan,Wang Chuan-Pi,Liu Xin. 2015

[8]Simultaneous Determination of 3 Kinds of Isomers of Clorprenaline and Baclofen Residues in Feed by Ultra Performance Liquid Chromatography-Tandem Mass spectrometry. Li Yang,Su Xiao-Ou,Wang Pei-Long,Fan Xia,Wang Rui-Guo,Wang Xiao. 2014

[9]Dissipation, transfer and safety evaluation of emamectin benzoate in tea. Chen, Zongmao.

[10]Simultaneous Determination of Plant Growth Regulators and Imidacloprid, Acetamiprid in Tea by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry. Zhu Li,Wang Chen,Chen Hong-Ping,Zhang Ying-Bin,Zhou Su-Juan,Wang Guo-Qing,Liu Xin. 2017

[11]Determination of Aflatoxin B-1 and Aflatoxin B-2 in Edible Oil by Using Graphene Oxide-SiO2 as Soild Phase Extraction Coupled with HPLC. Wang Heng-Ling,Yu Li,Li Pei-Wu,Li Min,Zhang Qi,Zhang Wen,Wang Heng-Ling,Yu Li,Li Pei-Wu,Li Min,Zhang Wen,Wang Heng-Ling,Li Pei-Wu,Li Min,Zhang Qi,Yu Li,Li Pei-Wu,Zhang Qi. 2014

[12]Simultaneous determination of triazine herbicides in rice by high-performance liquid chromatography coupled with high resolution and high mass accuracy hybrid linear ion trap-orbitrap mass spectrometry. Mou, Ren-Xiang,Chen, Ming-Xue,Cao, Zhao-Yun,Zhu, Zhi-Wei.

[13]Determination of Tetracyclines and Their Epimers in Agricultural Soil Fertilized with Swine Manure by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry. Zheng Wen-li,Zhang Li-fang,Zhang Ke-yu,Wang Xiao-yang,Xue Fei-qun. 2012

[14]Silica/graphene oxide nanocomposites: Potential adsorbents for solid phase extraction of trace aflatoxins in cereal crops coupled with high performance liquid chromatography. Yu, Li,Ma, Fei,Ding, Xiaoxia,Wang, Hengling,Li, Peiwu,Yu, Li,Ma, Fei,Li, Peiwu,Yu, Li,Ma, Fei,Li, Peiwu,Yu, Li,Ding, Xiaoxia,Li, Peiwu,Ma, Fei,Ding, Xiaoxia,Wang, Hengling,Li, Peiwu. 2018

[15]Assessment of primary and secondary amine adsorbents and elution solvents with or without graphitized carbon for the SPE clean-up of food extracts in pesticide residue analysis. He, Yan,Liu, Yan-Hong. 2007

作者其他论文 更多>>
置顶
购物车
反馈

© 京ICP备09089781号-29 主办单位：中国农业科学院

学术资源： 中国农业科学院 农业专业知识服务系统 农科联盟资源共建共享平台 中国农业科技文献与信息服务平台 中国农业期刊集成服务平台