Natural surfactant used as an additive in the homogenate-ultrasound-synergistic extraction of regaloside A and polysaccharides from Lilium lancifolium bulbs using Doehlert matrix design
文献类型： 外文期刊
作者： Zhang, Aoqi 1 ; Zhao, Ru 1 ; Wang, Yunxia 1 ; Liu, Tingting 3 ; Tian, Hao 4 ; Yin, Xing 1 ; Yang, Lei 1 ; Sui, Xiaoyu 3 ;
作者机构： 1.Northeast Forestry Univ, Coll Chem Chem Engn & Resource Utilizat, Harbin 150040, Peoples R China
2.Nanjing Xiaozhuang Univ, Key Lab Qual & Safety Agr Prod Nanjing, Nanjing 211171, Peoples R China
3.Qiqihar Med Univ, Coll Pharm, Qiqihar 161006, Peoples R China
4.Yunnan Acad Agr Sci, Inst Agroprod Proc, Kunming 650223, Yunnan, Peoples R China
5.Heilongjiang Prov Key Lab Ecol Utilizat Forestry, Harbin 150040, Peoples R China
6.Northeast Forestry Univ, Key Lab Forest Plant Ecol, Minist Educ, Harbin 150040, Peoples R China
关键词： Lilium lancifolium; Homogenate-ultrasound-synergistic extraction; Regaloside A; Polysaccharides; n-hexyl glucoside; Natural surfactant
期刊名称：INDUSTRIAL CROPS AND PRODUCTS （ 影响因子：6.449； 五年影响因子：6.508 ）
ISSN： 0926-6690
年卷期： 2022 年 188 卷
页码：
收录情况： SCI
摘要： In this study, 10 different natural surfactants were compared as additives for the simultaneous extraction of lipophilic regaloside A and water-soluble polysaccharides from tiger lily (Lilium lancifolium Thunb.) bulbs by homogenate-ultrasound-synergistic extraction. Four significant factors that affect the yields of regaloside A and polysaccharides, including homogenate speed, ultrasound irradiation power, reaction temperature and ultrasound irradiation time, were screened by single-factor experiments and Plackett-Burman design and then optimized using Doehlert matrix design combined with a desirability function. The optimal extraction process conditions were obtained as follows: APG06 (n-hexyl glucoside) surfactant concentration of 0.6%, homogenate speed of 20000 r/min, homogenate time of 6 min, liquid-solid ratio of 20 mL/g, ultrasound irradiation power of 300 W, ultrasound irradiation time of 52 min, reaction temperature of 62.8 degrees C, and buffer and cavitation times of 1.5 s and 2.0 s, respectively. Under the optimal extraction conditions, regaloside A and polysaccharides yields of 2.797 +/- 0.084 mg/g and 0.493 +/- 0.016 g/g are obtained with relative standard deviations of 3.00% and 3.50%, respectively. The results of the method validation and comparison with the conventional method show that homogenate-ultrasound-synergistic extraction with APG06 as an additive is a green, efficient and energy-saving extraction method. Compared with the traditional extraction method, HUSE with APG06 as an additive is an effective method to extract regaloside A and polysaccharides from L. lancifolium bulbs. This study provides a reference for the development of green low carbon natural product extraction process.
- 相关文献
作者其他论文 更多>>
-
Preparation and characterization of a modified Canna starch as a wall material for the encapsulation of methyleugenol improves its antifungal activity against Fusarium trichothecioides
作者：Xiao, Yao;Yang, Lei;Liu, Tingting;Liu, Zaizhi;Gu, Huiyan;Yang, Lei;Liu, Tingting;Tian, Hao
关键词：Microcapsules; Antifungal activity; Modified Canna starch; Methyleugenol
-
The dual effects of Congea chinensis Moldenke on inhibiting tumor cell proliferation and delaying aging by activating TERT transcriptional activity
作者：Peng, Lei;Dan, Juhua;Huang, Wenhui;Sang, Lei;Liu, Jing;Luo, Ying;Tian, Hao;Li, Zhiming;Li, Wanyi;Luo, Ying;Liu, Jing;Li, Wanyi
关键词：Congea chinensis Moldenke; Cytotoxic antitumor activity; Apoptosis; TERT
-
13-Cyclodextrin as a booster for ultrasound-assisted extraction of secoiridoids from Gentiana rigescens using a biobased deep eutectic solvent
作者：Yang, Yang;Gao, Hongfei;Wang, Zehao;Yang, Lei;Fan, Changwen;Zhao, Ru;Ruan, Ming;Gu, Huiyan;Yang, Lei;Tian, Hao;Liu, Tingting
关键词：Cyclodextrin; Biobased deep eutectic solvent; Gentiana rigescens Franch. ex Hemsl; Secoiridoid; Ultrasound-assisted extraction
-
Mitochondrial transplantation ameliorates hippocampal damage following status epilepticus
作者：Jia, Xiaoxia;Wang, Qinghua;Ji, Jianlun;Guo, Lin;Wang, Yun;Lu, Wenchun;Liu, Zhidong;Guo, Lin;Tian, Hao;Guo, Lin;Wang, Yun
关键词：cognitive deficit; emotional disorders; hippocampal damage; mitochondrial transplantation; status epilepticus
-
An efficient approach to obtain essential oil, oleanoic acid, 3-O-acetyloleanolic acid and betulinic acid from fresh leaves of Melaleuca bracteata F. Muell. 'Revolution Gold' using microwave and gravity-assisted solvent-free distillation followed by extraction
作者：Gao, Hongfei;Fan, Changwen;Yang, Yang;Wang, Zehao;Yang, Lei;Zhao, Ru;Gu, Huiyan;Yang, Lei;Tian, Hao;Zhang, Qiang;Zhang, Xiaonan
关键词：Melaleuca bracteata; Microwave gravity-assisted solvent-free distil-lation followed by extraction; Essential oil; Oleanoic acid; 3-O-acetyloleanolic acid; Betulinic acid
-
The sigma-1 receptor-TAMM41 axis modulates neuroinflammation and attenuates memory impairment during the latent period of epileptogenesis
作者：Ji, Jianlun;Liu, Zhidong;Guo, Lin;Ji, Jianlun;Gao, Ce;Wang, Qinghua;Jia, Xiaoxia;Wei, Yaqin;Liu, Zhidong;Wang, Yun;Guo, Lin;Tian, Hao;Wang, Yun;Guo, Lin
关键词：epileptogenesis; memory impairment; mitochondrial translocator assembly and maintenance 41 homolog; neuroinflammation; sigma-1 receptor
-
Ion-Modified Starch Film Enables Rapid Detection of Spoiled Fruit Juices
作者：Qin, Shijiao;Wu, Yujia;Liu, Yun;Kan, Huan;Hou, Defa;Lin, Xu;Zheng, Yunwu;Liu, Can;Tian, Hao;Zheng, Zhifeng
关键词：ion modified; starch film; drink spoilage; pH response; rapid determination
