您好，欢迎访问中国农业科学院 机构知识库！

全部

  • 全部
  • 标题
  • 学者
  • 机构
  • 关键词

Simultaneous Determination of Plant Growth Regulators in Fruit by Ultra-performance Liquid Chromatography-Tandem Mass Spectrometry Coupled with Modified QuEChERS Procedure

文献类型： 外文期刊

作者： Yan Zhen 1 ; Nie Ji-Yun 1 ; Cheng Yang 1 ; Li Zhi-Xia 1 ; Xu Guo-Feng 1 ; Li Hai-Fei 1 ;

作者机构： 1.Chinese Acad Agr Sci, Inst Pomol, Qual Inspect & Test Ctr Fruit & Nursery Stocks, Minist Agr,Lab Qual & Safety Risk Assessment Frui, Xingcheng 125100, Peoples R China

关键词： Ultra-performance liquid chromatography-tandem mass spectrometry;Plant growth regulators;Fruit

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2017 年 45 卷 5 期

页码：

收录情况： SCI

摘要： Five plant growth regulators, uniconazole, 6-benzyladenine, kinetin, 4-chlorophenoxyacetic acid and diethyl aminoethyl hexanoate, frequently used in apple, grape, strawberry, peach and orange, were determined by ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). A modified QuEChERS (Quick, easy, cheap, effective, rugged and safe) procedure was used in sample pretreatment, which involved extraction with acetonitrile containing 1% acetic acid and clean-up with a mixture of ODS and MgSO4. Mass spectrometric determination was performed in multiple reaction monitoring mode (MRM) using external standards for calibration. The results indicated that the calibration curves for the target analytes were linear in the range of 1-100 mu g L-1 with correlation coefficients greater than 0.999. The recoveries at three spiked levels ranged from 71.82% to 109.24% with RSDs from 0.57% to 12.43%. The respective limits of detection (LOD) and limits of quantification ( LOQ) were 0.15-0.45 mu g kg(-1) and 0.51-1.50 mu g kg(-1) for uniconazole, 0.28-0.53 mu g kg(-1) and 0.94-1.75 mu g kg(-1) for 6-benzyladenine (6-BA), 0.15-69 mu g kg(-1) and 0.51-2.29 mu g kg(-1) for kinetin (6-KT), 0.22-0.60 mu g kg(-1) and 0.74-2.01 mu g kg(-1) for 4-chlorophenoxyacetic acid (4-CPA), 0.88-1.89 mu g kg(-1) and 2.89-6.29 mu g kg(-1) for diethyl aminoethyl hexanoate (DA-6).

  • 相关文献

[1]流星雨无籽西瓜新品种的选育. 刘文革,阎志红,赵胜杰,何楠,谭素英. 2009

[2]纯黑大果无籽西瓜新品种郑抗无籽5号的选育. 刘文革,谭素英,阎志红,何楠,赵胜杰. 2009

[3]Determination of a novel paclitaxel derivative (NPD-103) in human plasma by ultra-performance liquid chromatography-tandem mass spectrometry. Zhang, Shuang-Qing,Chen, Guo-Hua. 2009

[4]Brain Concentration of Ginsenosides and Pharmacokinetics after Oral Administrationof Mountain-cultivated Ginseng. Li, Meijia,Guan, Yiming,Liu, Ning,Shao, Cai,Liu, Zhengbo,Chen, Jianbo,Wang, Qiuxia,Pan, Xiaoxi,Sun, Hai,Zhang, Yayu. 2017

[5]Sensitive detection of beta-agonists in pork tissue with novel molecularly imprinted polymer extraction followed liquid chromatography coupled tandem mass spectrometry detection. Wang, Peilong,Su, Xiaoou,Liu, Ximeng,Zhu, Ruohua.

[6]Simultaneous Determination of Five Plant Growth Regulators in Fruits by Modified Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) Extraction and Liquid Chromatography-Tandem Mass Spectrometry. Shi, Xiaomei,Jin, Fen,Huang, Yuting,Du, Xinwei,Wang, Miao,Shao, Hua,Jin, Maojun,Wang, Jing,Li, Chunmei.

[7]Exogenous Application of Abscisic Acid, Putrescine, or 2,4-Epibrassinolide at Appropriate Concentrations Effectively Alleviate Damage to Tomato Seedlings from Suboptimal Temperature Stress. Jiang, Weijie,Bai, Jie,Yang, Xueyong,Yu, Hongjun,Liu, Yanpeng.

[8]EFFECTS OF SOIL DROUGHT STRESS ON PLANT REGENERATION EFFICIENCY AND ENDOGENOUS HORMONE LEVELS OF IMMATURE EMBRYOS IN WHEAT (&ITTRITICUM AESTIVUM&IT L.). Bie, Xiaomin,Wang, Ke,Liu, Chang,Du, Lipu,Mao, Xinguo,Ye, Xingguo,Bie, Xiaomin,Liu, Yongwei. 2017

[9]Plantlet Regeneration of Tartary Buckwheat (Fagopyrum tataricum Gaertn.) in Vitro Tissue Cultures. Wang, Cheng-Long,Dong, Xue-ni,Ding, Meng-qi,Shao, Ji-Rong,Wang, Cheng-Long,Dong, Xue-ni,Ding, Meng-qi,Tang, Yi-Xiong,Wu, Yan-Min,Zhou, Mei-Liang,Zhu, Xue-Mei.

[10]High Frequency Adventitious Shoot Induction and Plant Regeneration from Hypocotyl of Ramie [Boehmeria nivea (L.) Gaud]. Ma, Xiongfeng,Yu, Chunming,Tang, Shouwei,Wang, Yanzhou,Zhu, Aiguo,Zhu, Siyuan,Gong, Benhe,Xiong, Heping. 2010

[11]Analysis on Current Fruit Market and Late Concerns in China. Junye Zhao,Qiao Zhang. 2014

[12]Analysis on Current Fruit Market and Late Concerns in China. ZHAO Junye,ZHANG Qiao. 2013

[13]Speciation analysis of arsenic in fruits and vegetables by high performance liquid chromatography-hydride generation-atomic fluorescence spectrometry with ultrasonic extraction. Shouhui Dai,Min Wang,Jing Qiu,Hui Yang,Fuhua Wang. 2011

[14]Cloning and characterization of CaGID1s and CaGAI in Capsicum annuum L.. Cao Ya-cong,Sul Xiao-lei,Zhang Zhen-xian,Cao Ya-cong,Zhang Zheng-hai,Wang Li-hao,Zhang Bao-xi. 2016

[15]Characterization of 1-aminocyclopropane-1-carboxylic acid synthase (ACS) genes during nectarine fruit development and ripening. Zeng, Wenfang,Pan, Lei,Liu, Hui,Niu, Liang,Lu, Zhenhua,Cui, Guochao,Wang, Zhiqiang. 2015

[16]Characterization and expression profiling of cucumber kinesin genes during early fruit development: revealing the roles of kinesins in exponential cell production and enlargement in cucumber fruit. Yang, Xue Yong,Wang, Yan,Jiang, Wei Jie,Liu, Xiao Ling,Zhang, Xiao Meng,Yu, Hong Jun,Huang, San Wen,Liu, Guo Qin. 2013

[17]Rapid Analysis of Tetraconazole Residues in Fruits and Vegetables using Ethyl Acetate Extraction and Gas Chromatography-tandem Mass Spectrometry. Doug, Fengshou,Liu, Xingang,Li, Jing,Li, Yuanbo,Zheng, Yongquan,Shan, Weili.

[18]Research on Fruit Market Price Risk Thresholds in China. Zhao, Junye,Zhang, Qiao,Zhao, Junye,Zhang, Qiao. 2014

[19]Predicting oleocellosis sensitivity in citrus using VNIR reflectance spectroscopy. Zheng, Yongqiang,He, Shaolan,Yi, Shilai,Deng, Lie,Zheng, Yongqiang,Zhou, Zhiqin,Mao, Shasha,Zhao, Xuyang. 2010

[20]Nondestructive Examination of Tomato Chilling Injury by Ultraweak Luminescence. Zhao Dan-ying,Sheng Ji-ping,Ding Yang,Shen Lin,Liu Can,Zhao Dan-ying,Sheng Ji-ping,Fan Bei. 2010

作者其他论文 更多>>
置顶
购物车
反馈

© 京ICP备09089781号-29 主办单位：中国农业科学院

学术资源： 中国农业科学院 农业专业知识服务系统 农科联盟资源共建共享平台 中国农业科技文献与信息服务平台 中国农业期刊集成服务平台