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Multi-residue analytical method development and dietary exposure risk assessment of 345 pesticides in mango by LC-Q-TOF/MS

文献类型： 外文期刊

作者： Wu, Xingqiang 1 ; Li, Jianxun 3 ; Wei, Jing 2 ; Tong, Kaixuan 1 ; Xie, Yujie 1 ; Chang, Qiaoying 1 ; Yu, Xiaoxuan 1 ; Li, Bei 2 ; Lu, Meiling 4 ; Fan, Chunlin 1 ; Chen, Hui 1 ;

作者机构： 1.Chinese Acad Inspect & Quarantine, Key Lab Food Qual & Safety State Market Regulat, Beijing 100176, Peoples R China

2.Hainan Inst Food Control, Key Lab Trop Fruits & Vegetables Qual & Safety Sta, Haikou 570314, Peoples R China

3.Chinese Acad Agr Sci, Inst Food Sci & Technol, Beijing 100193, Peoples R China

4.Agilent Technol China Ltd, Beijing 100102, Peoples R China

关键词： Mango; LC-Q-TOF/MS; QuEChERS; Pesticide residues; Risk assessment

期刊名称：FOOD CONTROL （ 影响因子：6.3； 五年影响因子：6.1 ）

ISSN： 0956-7135

年卷期： 2025 年 170 卷

页码：

收录情况： SCI

摘要： Mango is attracting increasing global attention for its superior flavor and nutritional benefits. However, the use of pesticides has resulted in a threat to its quality, safety, and human health due to their inevitable residue. There is an urgent need for advanced technologies that can efficiently and sensitively analyze a wide range of pesticides. In this study, a high-throughput screening and quantification method for 345 pesticides in mango was established by applying a modified QuEChERS method combined with liquid chromatography-quadrupole-timeof-flight mass spectrometry (LC-Q-TOF/MS). A response surface methodology (RSM) optimized the critical parameters for extracting various pesticides in 1% acetic acid-acetonitrile (v/v) using MgSO4, PSA, C18, and GCB as the adsorbents. The proposed method was successfully validated and applied to the quantitative detection of pesticide residues in 73 mango samples from Hainan. The study found pesticide residues in 95.9% of mango samples, of which 3 samples had residue concentrations in excess of the Chinese maximum residue limit. A total of 24 pesticides were detected, with detection percentages ranging from 1.4% (Thiabendazole) to 41.1% (Pyraclostrobin). Considering the possible health risks related to pesticide residues, risk assessment of human exposure to pesticides via intake of mango was evaluated. The acute and chronic dietary exposure risks related to pesticide residues in mango were accepted. In conclusion, this study provides a powerful platform for monitoring multiple pesticides in mango. First, it can promote the rational use of pesticides, and second, it can help consumers to assess the risk of dietary exposure to pesticide residues.

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