Multiresidue determination of 19 anabolic steroids in animal oil using enhanced matrix removal lipid cleanup and ultrahigh performance liquid chromatography-tandem mass spectrometry
文献类型： 外文期刊
作者： Yu Jiafeng 1 ; Suo Decheng 2 ; Lei Xiaoyong 3 ; Li Yang 2 ; Lin Guangyu 3 ; Bi Su Min 4 ;
作者机构： 1.Liaoning Prov Inspect & Testing Certificat Ctr, Shenyang 110016, Peoples R China
2.Chinese Acad Agr Sci, Inst Qual Stand & Testing Technol Agr Prod, Beijing 100081, Peoples R China
3.Liaoning Agr Dev Serv Ctr, Shenyang 110032, Peoples R China
4.Shenyang Social Welf Inst, Shenyang 110165, Peoples R China
期刊名称：ANALYTICAL METHODS （ 影响因子：2.596； 五年影响因子：2.296 ）
ISSN： 1759-9660
年卷期：
页码：
收录情况： SCI
摘要： A method for sensitive analysis of 19 anabolic steroids (AS) in animal oil using enhanced matrix removal lipid (EMR-Lipid) cleanup and ultrahigh performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS) was developed. Oil samples were extracted with 20 mL of acetonitrile aqueous solution and purified using EMR-Lipid cartridges. The eluent was evaporated to dryness under nitrogen and analyzed by UHPLC-MS/MS using 0.1% formic acid-acetonitrile and 0.1% formic acid-water solutions as the mobile phase via gradient elution. The method effectively removed unwanted matrix co-extractives better than other extraction cleanup techniques while still delivering acceptable recovery results for most of the AS. The established quantification method showed AS recovery in the range of 72.9-110.7% with good precision (relative standard deviation < 15%).
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